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    Investigation 
of
 Interactions 
between 
β‐blocker
 Drugs 
and
 Polymers 
via
 NMR
 Diffusion
 Experiments


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    Marble.pdf (519.8Kb)
    Date
    2010-09-09
    Author
    Marble, Sarah
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    Subjects
    NMR; spectroscopy
    Abstract
    NMR spectroscopy was used to study the binding of β-blockers to chiral polymers. In order to effectively separate these mixtures, the chiral interactions need to be well understood. Chiral polymers were used to study binding constants and free energy values for each analyte. The Propranolol had the strongest interaction with each polymer while Atenolol had the weakest. Correlations were seen between NMR association constants and chromatographic retention times as well as between the NMR free energies of binding and chiral selectivities. It was also concluded the polymer forms a chiral pocket with which the analytes interact
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